| Title: | Development of methods for field determination of chromium (VI) in water and groundwater |
| Author: | |
| Document Type: | Thesis |
| Department: | Department of Chemical Engineering, Chemistry and Environmental Science |
| Degree: | Master of Science |
| Major: | Environmental Science |
| Advisory Committee: |
Kebbekus, Barbara B.
Ososkov, Victor
Mitra, S.
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| Thesis Date: | 1997, May |
| Keywords: |
Water --Analysis.
Trace elements --Analysis.
Chromium --Toxicology.
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| Availability: | Unrestricted |
| Abstract: |
In this study, methods for the determination of chromium (VI) in fresh
water at low ppb levels for the use under field conditions were developed. The
plan was to devise a simple and inexpensive on-site field method which
would be useable by people who are not professional chemists. An investigation
was carried out to develop a preconcentration and determination procedure
for the analysis of chromium (VI) using anion-exchange membranes and/or
resins. The chromium (VI) would be sorbed to the solid support and then
treated with 1 ,5-diphenylcarabzide, a specific colorimetric reagent
for chromium (VI), which forms a red complex upon reaction. A simple
preconcentration procedure, and a portable colorimeter were used to
make the method suitable for field use. Sensitivity, selectivity and
precision are evaluated to ensure that the method to provides accurate
and reliable results in the field.
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| Complete Thesis: |
njit-etd1997-028
(85 pages ~ 3,738 KB pdf)
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